|
( d6 A* Q( d3 l; A
gHMQC . M6 {* F; w$ c- r
Relax. delay 1.000 sec ' K4 ]* D, _# P9 }5 T& O2 x) s
Acq. time 0.160 sec ) E( s/ {; J# Z" b
width 6402.6 Hz
% `# Q/ ^; l* k o5 M2D width 17105.0 Hz
' ^* a6 S, F7 B7 [2 n) c; k" M32 repetitions
$ D6 g4 I: p! Y- I2×256 increments ) g( E1 t# Q- m0 D! ~1 `+ a
OBSERVE H1, 400.1596234 MHz
5 i2 k/ k- F, E7 w5 UDECOUPLE C13, 100.6277427 MHz $ ~+ X! D _- D: F
POWER 44 dB
: J9 y; m1 e& ], Won during acquisition 4 B* e {$ S ]& s/ S6 O* m/ p
off during delay 1 h7 @* C1 ~0 e x2 [9 Z& l
GARP-1 modulated 1 W1 [# s% {9 k+ S8 A/ W& Y% J
DATE PROCESSING 1 V; a& o! ?& G4 i
Gauss apodization 0.074 sec
% y( h% Q2 Y1 bF1 DATE PROCESSING 5 X3 K1 `( A, P& L
Gauss apodization 0.014 sec 8 [: W+ _ v+ u. N
FT size 2048×2048
/ q- `& G7 s* k4 n4 STotal time 5 hr, 33 min,23 sec 0 g4 ^3 ?" B8 q
( Z9 V7 \& S a $ q4 s4 M3 Q# h3 w' p" X) ]4 S
gHMBC
, d! }) V4 @, Y" @1 NRelax. delay 1.000 sec ) Q: D6 Z! y4 @6 C! M/ @; w1 s
Acq. time 0.160 sec
; U4 Y7 e8 F5 W' w% p$ zwidth 6402.6 Hz 6 x8 h! Y' T4 A
2D width 24147.3 Hz - \ E* G6 x$ \& g3 G
32 repetitions & v4 K7 j" V6 o E4 n* {
512 increments + `9 Z1 \( v. a4 D
OBSERVE H1, 400.1596234 MHz ' D# f, X' X' f' p1 v7 v
DATE PROCESSING 7 ?- i5 N6 }/ h& Q
Sine bell 0.080 sec
+ z" c3 N {- H9 pF1 DATE PROCESSING
/ y: g9 O7 n, \# i! K+ L) CSine bell 0.008 sec 4 ?5 g+ U |; [/ \7 r% S$ I) M
FT size 2048×2048 2 I' Q7 g; c+ O( c4 A% A1 i' S
Total time 5 hr, 42 min, 37 sec
) K" k; G) ?- ?1 |1 w- T想问一下，从上述参数中可以看出D1指的是什么，还有是弛豫间隔和NS都是什么啊，不是学这个的，不太懂，还请内行帮忙,先谢谢了 | 
楼主: celan
发表于 2009-1-29 21:22:58
